Synthesis of Transition Metal Complexes of Schiff Base by Ultrasound Irradiation Method and Conventional Method- A Comparative Study |
Author(s): |
Datal Chaitanya Atmaram , Dayanand Science College, Latur; Akash Singare, SRTMUN University,Nanded; Jaiprakash Dargad, Dayanand Science College, Latur; Nanda Korde, Dayanand Science College, Latur |
Keywords: |
Ultrasonication, Metal Complexes, Time, Yield, Salicylaldehyde, Anthranilic Acid, Purity, Organic Reaction |
Abstract |
Ultrasound irradiation has allowed preparation of the synthesized product along good yield in extremely short reaction period. The quality of the product was determined by SEM- TEM, HNMR, CMR etc. The high intensity ultrasound is regarded as an easy environmentally-friendly and flexible synthetic instrument compounds of co-ordination. The ultrasonication supply the synthesized molecule in excessive yield and clarity in shorter reaction time differentiated along the conventional method. Ultrasound irradiation extensively utilized in the preparation of nano particles and polymer supported material. The reaction are selected that requires additional stirring for accomplishment and fulfilled the ordinary temperature through the conventional method correlated along the ultrasound irradiation technique. Ultrasound technique is an supportive also in photosynthesis of nano complex can be extremely interesting for manufacturing function. In actual fact chemical changes in the period ultrasonic irradiation can also be helpful certain areas of chemical synthesis. Time for the reaction was very much less through ultrasound irradiation and the amount of product of reaction was too dominant as differentiated to the conventional method using reflux condition. The incorporate Schiff base and our metal complexes remain distinguish by the spectroscopic technique like UV-Visible, IR, and 1H NMR. The prepared Schiff base and there metal complexes showed satisfactory antimicrobial activity. |
Other Details |
Paper ID: IJSRDV11I50092 Published in: Volume : 11, Issue : 5 Publication Date: 01/08/2023 Page(s): 154-156 |
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