A Convenient Synthesis and Spectral Studies of 2-(2,2-Difluoroethoxy)-N-(6-Methylbenzo[D] Thiazole-2-Yl)-6-(Trifluoromethyl)Benzenesulfonamide |
Author(s): |
| Aakash Kumar , Research Scholar, Shri Venkateshwara University, Gajraula, Amroha, (U.P.), India |
Keywords: |
| 4-methylaniline, 2-Amino-6-methylbenzothiazole, sodium thiocyanate, sulfuryl chloride, pyridine, dichloromethane, 2-(2,2-difluoroethoxy)-6-(trifluoromethyl) benzene-1-sulfonyl chloride, 2-(2,2-difluoroethoxy)-N-(6-methylbenzo[d]thiazole-2-yl)-6(trifluoromethyl) benzenesulfonamide |
Abstract |
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4-methylaniline in chlorobenzene reacted with sulphuric acid, sodium thiocyanate and sulfuryl chloride to give 2-amino-6-methyl benzothiazole. This 2-amino-6-methyl benzothiazole was later further reacted with 2-(2,2-difluoroethoxy)-6-(trifluoromethyl)benzene-1-sulfonyl chloride in the presence of Dichloromethane and anhydrous Pyridine to afford 2-(2,2-difluoroethoxy)-N-(6-methylbenzo[d]thiazole-2-yl) 6(trifluoromethyl) benzenesulfonamide. |
Other Details |
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Paper ID: IJSRDV5I11019 Published in: Volume : 5, Issue : 1 Publication Date: 01/04/2017 Page(s): 1305-1307 |
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